反应条件
1: (COCl)2, DMSO / CH2Cl2 / 0.5 h / -78 °C 2: tetrahydrofuran; hexane / 1.) -78 deg C, 4 h, 2.) from -78 deg C to rt, overnight View Scheme
参考文献
Williams, Peter D.; Perlow, Debra S.; Payne, Linda S.; Holloway, M. Katharine; Siegl, Peter K. S.; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 3 p. 887 - 900
