1,3-双(4-甲氧基苯基)脲合成路线 （共 75 条）
反应条件
chlorine; tetrachloroethane, 1,1,2,2- Erhitzen des Reaktionsprodukts mit wss. Ammoniak auf 150-160grad;
参考文献
Shepard; Shonle
Journal of the American Chemical Society, 1948 , vol. 70, p. 1979
Full Text View citing articles Show Details
Imp.Chem.Ind.
Patent: US2046375 , 1932 ;
反应条件
carbon dioxide; oxygen; potassium iodide; PdI2 in ethylene glycol dimethyl ether
T=100°C; P=45600 Torr; 15 h;
参考文献
Gabriele, Bartolo; Mancuso, Raffaella; Salerno, Giuseppe; Costa, Mirco
Chemical communications (Cambridge, England), 2003 , # 4 p. 486 - 487
反应条件
dodecacarbonyltriiron; carbon monoxide; hydrogen; sodium methylate in tetrahydrofuran
T=60°C; P=760 Torr;
参考文献
Alper, Howard; Hashem, Khaled E.
Journal of the American Chemical Society, 1981 , vol. 103, # 21 p. 6514 - 6515
反应条件
sodium hydrogencarbonate in dichloromethane; water
12 h; Inert atmosphere;
参考文献
Roychowdhury, Additi; Ghosh, Pritam; Saha, Sourav Kr.; Mitra, Partha; Banerjee, Priyabrata
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2014 , vol. 124, p. 492 - 499
反应条件
dodecacarbonyltriiron; hydrogen; sodium methylate in tetrahydrofuran
T=60°C; P=760 Torr;
参考文献
Alper, Howard; Hashem, Khaled E.
Journal of the American Chemical Society, 1981 , vol. 103, # 21 p. 6514 - 6515
反应条件
potassium hydroxide; selenium in water; N,N-dimethyl-formamide
T=95°C; 13 h; atmospheric pressure;
参考文献
Wang, Xiaofang; Lu, Shiwei; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 8 p. 929 - 932
反应条件
tert.-butylhydroperoxide; iron(II) sulfate in water
T=20 - 80°C; under open air;
参考文献
Wei, Ying; Ding, Hongqian; Lin, Shaoxia; Liang, Fushun
Organic Letters, 2011 , vol. 13, # 7 p. 1674 - 1677
反应条件
in pyridine; water
T=20°C; Condensation; 2 h;
参考文献
Blanco, Jose L. Jimenez; Barria, Claudio Saitz; Benito, Juan M.; Mellet, Carmen Ortiz; Fuentes, Jose; Santoyo-Gonzales, Francisco; Fernandez, Jose M. Garcia
Synthesis, 1999 , # 11 p. 1907 - 1914
反应条件
1: carbon dioxide; 4-methoxy-aniline in dimethyl sulfoxide
T=20°C;
2: 4-methoxy-aniline With triphenylphosphine; diethylazodicarboxylate in dimethyl sulfoxide
T=20°C; 3 h; chemoselective reaction;
参考文献
Chaturvedi, Devdutt; Mishra, Nisha; Mishra, Virendra
Monatshefte fur Chemie, 2008 , vol. 139, # 3 p. 267 - 270
反应条件
dodecacarbonyltriiron; hydrogen in tetrahydrofuran
T=60°C; P=760 Torr;
参考文献
Alper, Howard; Hashem, Khaled E.
Journal of the American Chemical Society, 1981 , vol. 103, # 21 p. 6514 - 6515
