1,3-双(4-甲氧基苯基)脲合成路线 （共 75 条）
反应条件
in tetrahydrofuran
robotic synthesis; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Linclau, Bruno; Sing, Ashvani K.; Curran, Dennis P.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2835 - 2842
反应条件
in tetrahydrofuran
robotic synthesis; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Linclau, Bruno; Sing, Ashvani K.; Curran, Dennis P.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2835 - 2842
反应条件
benzene; dodecacarbonyltetrarhodium(0)
T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
参考文献
Naegeli; Tyabji; Conrad
Helvetica Chimica Acta, 1938 , vol. 21, p. 1127,1139
反应条件
T=230 - 240°C; 0.5 h;
参考文献
Hassan, Alaa A; Mourad, Aboul-fetouh E
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 277 - 279
Title/Abstract Full Text Show Details
Hassan, Alaa A.; Mourad, Aboul-Fetouh E.
Revue Roumaine de Chimie, 1994 , vol. 39, # 4 p. 397 - 404
反应条件
in tetrahydrofuran
robotic synthesis; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Linclau, Bruno; Sing, Ashvani K.; Curran, Dennis P.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2835 - 2842
反应条件
T=200 - 210°C; 0.75 h;
参考文献
Aly, N. F.; Fahmy, A. F. M.; Baddawy, H. A.; Alkhateeb, A. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 489 - 490
反应条件
1.1: N-benzyl-N,N,N-triethylammonium chloride; sodium azide / toluene / 24 h / 20 °C
2.1: toluene / 22 h / 90 °C
3.1: sodium hydroxide / water / 20 °C
3.2: 0 °C
3.3: pH Ca. 4
View Scheme
参考文献
Groszek, Grazyna
Organic Process Research and Development, 2002 , vol. 6, # 6 p. 759 - 761
反应条件
1.1: toluene / 22 h / 90 °C
2.1: sodium hydroxide / water / 20 °C
2.2: 0 °C
2.3: pH Ca. 4
View Scheme
参考文献
Groszek, Grazyna
Organic Process Research and Development, 2002 , vol. 6, # 6 p. 759 - 761
反应条件
1: water / 6.67 h / 275 °C / |Inert atmosphere
2: water / 150 °C / |Green chemistry
View Scheme
参考文献
Medina-Ramos, Wilmarie; Mojica, Mike A.; Cope, Elizabeth D.; Hart, Ryan J.; Pollet, Pamela; Eckert, Charles A.; Liotta, Charles L.
Green Chemistry, 2014 , vol. 16, # 4 p. 2147 - 2155
