1,3-双(4-甲氧基苯基)硫脲合成路线 （共 26 条）
反应条件
1: basic lead carbonate; aqueous ethanol / 50 - 60 °C 2: aqueous ammonium polysulfide / 45 °C 3: concentrated sulfuric acid / und Erhitzen des Reaktionsgemisches mit Wasser View Scheme
参考文献
Ferber; Schmolke
Journal fuer Praktische Chemie (Leipzig), 1940 , vol. <2> 155, p. 234,238
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=20°C; 1 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 22 p. 2520 - 2524
反应条件
triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dichloromethane T=0°C; 0.166667 h;
参考文献
Chaudhari, Pramod S.; Dangate, Prasad S.; Akamanchi, Krishnacharya G.
Synlett, 2010 , # 20 art. no. D17910ST, p. 3065 - 3067
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=20°C; 1 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 22 p. 2520 - 2524
参考文献
Bollini, Mariela; Casal, Juan Jose; Alvarez, Diego E.; Boiani, Lucia; Gonzalez, Mercedes; Cerecetto, Hugo; Bruno, Ana Maria
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 4 p. 1437 - 1444
反应条件
iron; paraffin oil T=280 - 290°C;
参考文献
Bayer and Co.
Patent: DE259363 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 204
反应条件
potassium hydroxide
T=20°C; 0.666667 h; MillingGreen chemistry;
参考文献
Zhang, Ze; Wu, Hao-Hao; Tan, Ya-Jun
RSC Advances, 2013 , vol. 3, # 38 p. 16940 - 16944
反应条件
in acetonitrile
T=25°C; 0.166667 h; Milling;
参考文献
Strukil, Vjekoslav; Igrc, Marina D.; Fabian, Laszlo; Eckert-Maksic, Mirjana; Childs, Scott L.; Reid, David G.; Duer, Melinda J.; Halasz, Ivan; Mottillo, Cristina; Friscic, Tomislav
Green Chemistry, 2012 , vol. 14, # 9 p. 2462 - 2473
反应条件
sodium hydrogencarbonate in dichloromethane; water
T=0 - 20°C; 48.5 h; Inert atmosphere;
参考文献
Tripathi, Chandra Bhushan; Mukherjee, Santanu
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1592 - 1598
反应条件
2-chloro-1-methyl-pyridinium iodide in dimethyl sulfoxide
T=40°C; 0.0166667 h;
参考文献
Takikawa, Yuji; Inoue, Noriyuki; Sato, Ryu; Takizawa, Saburo
Chemistry Letters, 1982 , p. 641 - 642
