sodium tetrahydroborate in ethanol T=0°C; 2 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Hitchings, Gregory J.; Vernon, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1757 - 1763
sodium tetrahydroborate in ethanol T=0°C; 2 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hitchings, Gregory J.; Vernon, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1757 - 1763
1: 2) acetic anhydride / 1) THF, reflux, 2 h, 2) reflux, 2 h 2: NaBH4 / ethanol / 2 h / 0 °C View Scheme
参考文献
Hitchings, Gregory J.; Vernon, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1757 - 1763
1: acetic anhydride / 2 h / Heating 2: 2) acetic anhydride / 1) THF, reflux, 2 h, 2) reflux, 2 h 3: NaBH4 / ethanol / 2 h / 0 °C View Scheme
参考文献
Hitchings, Gregory J.; Vernon, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1757 - 1763
