1227476-15-4合成路线 （共 213 条）
参考文献
Emerson; Reed; Merner
Journal of the American Chemical Society, 1941 , vol. 63, p. 752
反应条件
hydrogen; nickel in methanol; water T=180°C; P=37503.8 Torr; 0.116667 h;
参考文献
Duslo, A.S. Sala
Patent: US6388136 B1, 2002 ;
Location in patent: Page column 13 ;
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol T=20°C; 5 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
hydrogenchloride; zinc(II) chloride T=35 - 40°C; unter Luftabschluss;
参考文献
Pummerer; Dally
Chemische Berichte, 1926 , vol. 59, p. 2176
反应条件
in benzene-d6 T=23°C; 1 h; Inert atmosphereSealed tube;
参考文献
Frazier, Brenda A.; Williams, Valerie A.; Wolczanski, Peter T.; Bart, Suzanne C.; Meyer, Karsten; Cundari, Thomas R.; Lobkovsky, Emil B.
Inorganic Chemistry, 2013 , vol. 52, # 6 p. 3295 - 3312
反应条件
1: fuming sulfuric acid / 130 °C 2: tin dichloride; hydrochloric acid View Scheme
参考文献
Laar
Chemische Berichte, 1881 , vol. 14, p. 1932
参考文献
Laar
Chemische Berichte, 1881 , vol. 14, p. 1932
反应条件
ethylene glycol dimethyl ether; lithium anschliessend Behandeln mit Dimethylsulfat;
参考文献
Reesor; Wright
Journal of Organic Chemistry, 1957 , vol. 22, p. 375,380
反应条件
1.1: Schlosser-Lochmann superbase n-BuLi/t-BuOK(LICKOR) / tetrahydrofuran / 2 h / -40 °C / |Inert atmosphere 1.2: 2 h / -40 °C / |Inert atmosphere 2.1: lithium diisopropyl amide / tetrahydrofuran / 2 h / -40 °C / |Inert atmosphere 2.2: |Inert atmosphere View Scheme
参考文献
Nguyen, Thi Thanh Thuy; Boussonniere, Anne; Banaszak, Estelle; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2775 - 2780
反应条件
potassium; dimethyl sulfate
参考文献
Reesor; Wright
Journal of Organic Chemistry, 1957 , vol. 22, p. 375,380
