1227476-15-4合成路线 （共 213 条）
反应条件
T=160 - 170°C; im geschlossenen Rohr;
参考文献
Becker
Chemische Berichte, 1887 , vol. 20, p. 2006
反应条件
1.1: hydrazine hydrate / ethanol / 0.5 h / 60 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 - -60 °C / Inert atmosphere 2.2: 1 h / -60 - 20 °C / Inert atmosphere 3.1: titanium(III) chloride; water / tetrahydrofuran / Reflux; Inert atmosphere View Scheme
参考文献
Zhang, Yan; Tang, Qiang; Luo, Meiming
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 13 p. 4977 - 4982
反应条件
Produkt5: Blausaeure; Produkt6: Ammoniak;
参考文献
Claus
Chemische Berichte, 1905 , vol. 38, p. 7
反应条件
1: chlorosulfuric acid / 125 °C 2: pyridine 3: tin; HCl; water View Scheme
参考文献
Journal of Organic Chemistry, , vol. 10, p. 205,208
反应条件
cesium hydroxide; anhydrous tetramethylammonium chloride in water T=80°C; P=760 Torr; 3 h; Product distribution / selectivity;
参考文献
Rains, Roger Keranen; Fields JR., Donald L.; Triplett II, Ralph Dale
Patent: US2004/39181 A1, 2004 ;
Location in patent: Page 10 ;
反应条件
cesium hydroxide; tetramethyl-ammonium fluoride T=80°C; P=20 Torr; 3 h; Azeotropic distillation; Product distribution / selectivity;
参考文献
US2004/39181 A1, ;
Page 14 ;
反应条件
ammonium formate; 1-n-butyl-3-methylimidazolium tetrafluoroborate; zinc in water T=20°C; 0.416667 h;
参考文献
Khan, Faiz Ahmed; Dash, Jyotirmayee; Sudheer; Gupta, Rakesh Kumar
Tetrahedron Letters, 2003 , vol. 44, # 42 p. 7783 - 7787
反应条件
aluminium telluride; water in tetrahydrofuran 0.333333 h; Heating;
参考文献
Angewandte Chemie, , vol. 92, # 12 p. 1042 - 1043
反应条件
1: Azobenzene With Schlosser-Lochmann superbase n-BuLi/t-BuOK(LICKOR) in tetrahydrofuran T=-40°C; 2 h; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran T=-40°C; 2 h; Inert atmosphere; Reagent/catalyst; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 79, # 6 p. 2775 - 2780
反应条件
borane-ammonia complex in acetonitrile T=40°C; 19 h; Inert atmosphere;
参考文献
Dunn, Nicole L.; Ha, Minji; Radosevich, Alexander T.
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11330 - 11333
