反应条件
Multi-step reaction with 6 steps 1: LDA / tetrahydrofuran; hexane / Ambient temperature2: diethyl ether3: 75 percent / NaOMe / methanol / 18 h / Heating4: 82 percent / air / ethanol; aq. NaOH / 24 h / Ambient temperature5: 0.41 g / 15percent HClO4 / 8 h / Heating6: 33 percent / BBr3 / CH2Cl2 / -78 deg C then r.t., 1 h
参考文献
Watanabe; Date; Furukawa Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 2 p. 292 - 297