3-(2-甲氧基苯基)苯甲醛合成路线 (共 4 条)
反应条件
potassium phosphate; [2-(dicylohexylphopshino)-2',6'-dimethoxybiphenyl-Pd]2*2BF4 in toluene T=70°C; Suzuki-Miyaura coupling; 1 h;
参考文献
Barder, Timothy E.
Journal of the American Chemical Society, 2006 , vol. 128, # 3 p. 898 - 904
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran; water; toluene T=105°C; Suzuki coupling; 36 h; Inert atmosphere;
参考文献
Hunter, Christopher A.; Misuraca, Maria Cristina; Turega, Simon M.
Journal of the American Chemical Society, 2011 , vol. 133, # 3 p. 582 - 594
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol T=100°C; Suzuki-Miyaura reaction; 4 h;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1075 - 1080
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI 1.) benzene/THF, 63 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848