Fishman, Andrew G.; Mallams, Alan K.; Rossman, Randall R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 787 - 798
Multi-step reaction with 3 steps 1: 45 percent / triethylamine (33percent) / methanol / 66 h / 25 °C2: 87 percent / acetone / 18 h / 25 °C3: 61 percent / N-(3-dimethylaminopropyl)-N'-ethylcarbodi-imide hydrochloride, pyridine, TFA / dimethylsulfoxide / 18 h / 25 °C
参考文献
Fishman, Andrew G.; Mallams, Alan K.; Rossman, Randall R. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 787 - 798
Multi-step reaction with 3 steps 1: 45 percent / triethylamine (33percent) / methanol / 66 h / 25 °C2: 87 percent / acetone / 18 h / 25 °C3: 37 percent / N-(3-dimethylaminopropyl)-N'-ethylcarbodi-imide hydrochloride, pyridine, TFA / dimethylsulfoxide / 19 h / 25 °C / chromatography on silica gel
参考文献
Fishman, Andrew G.; Mallams, Alan K.; Rossman, Randall R. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 787 - 798
