反应条件
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0.25 h / 20 °C / |Inert atmosphere 1.2: 20 °C / |Inert atmosphere 2.1: FeCl3·6H2O / dichloromethane; methanol / 0.5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Nadler, Andre; Reither, Gregor; Feng, Suihan; Stein, Frank; Reither, Sabine; Mueller, Rainer; Schultz, Carsten
Angewandte Chemie - International Edition, 2013 , vol. 52, # 24 p. 6330 - 6334
Angew. Chem., 2013 , vol. 125, # 24 p. 6455 - 6459,5