1228679-43-3合成路线 （共 12 条）
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: N-Methoxy-N-methyl-benzamide in tetrahydrofuran T=40°C; 1 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: N-methoxy-N-methylpropionamide in tetrahydrofuran T=40°C; 1 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: methyl iodide in tetrahydrofuran T=0°C; 1 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: CD3CON(OMe)Me in tetrahydrofuran T=0°C; 2 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: benzaldehyde in tetrahydrofuran T=-10°C; 0.5 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: iPrCON(OMe)Me in tetrahydrofuran T=40°C; 0.5 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: N-methoxy-N-methyl-2,2-dimethyl-propamide in tetrahydrofuran T=40°C; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: tBuCON(OtBu)Me in tetrahydrofuran T=40°C; 1 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: N,O-dimethylacetohydroxamic acid in tetrahydrofuran T=0°C; 2 h; 3: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: With water-d2 in tetrahydrofuran
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
