5β-雄烷-3,17-二酮合成路线 (共 14 条)
反应条件
potassium tri-sec-butyl-borohydride in tetrahydrofuran T=-75°C; 3 h;
参考文献
Goendoes, Gyoergy; Orr, James C.
Journal of the Chemical Society, Chemical Communications, 1982 , # 21 p. 1239 - 1240
反应条件
potassium tri-sec-butyl-borohydride in tetrahydrofuran T=22°C; 25 h; var. time, temp., amount of reagent; Product distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 21 p. 1239 - 1240
反应条件
trifluoroacetic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in o-di-fluorobenzene; dimethyl sulfoxide T=60°C; 40 h; Temperature; regioselective reaction;
参考文献
Iida, Takashi; Omura, Kaoru; Sakiyama, Ryou; Kodomari, Mitsuo
Chemistry and Physics of Lipids, 2014 , vol. 178, p. 45 - 51
反应条件
benzeneselenenyl chloride; dihydrogen peroxide Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Abul-Hajj, Yusuf J.
Journal of the Chemical Society, Chemical Communications, 1985 , # 21 p. 1479 - 1481