2,9-二氯-4,7-二苯基-1,10-菲啰啉合成路线 (共 2 条)
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane; water
T=80 - 100°C; Suzuki Coupling; Inert atmosphere;
参考文献
E.I.DU PONT DE NEMOURS AND COMPANY
Patent: US2012/65402 A1, 2012 ;
Location in patent: Page/Page column 14-15 ;
反应条件
With phosphorus pentachloride; trichlorophosphate 8 h; Inert atmosphereReflux; Show Experimental Procedure
参考文献
E.I.DU PONT DE NEMOURS AND COMPANY Patent: US2012/65402 A1, 2012 ; Location in patent: Page/Page column 13 ;