1: 78 percent / acetonitrile / 48 h / Ambient temperature 2: acetonitrile / 18 h / Ambient temperature 3: 60 percent / 2M NaOH / H2O / 0 °C View Scheme
参考文献
Gisby, Graham P.; Sammes, Peter G.; Watt, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 249 - 256
1: 2,3-dimethylbutane-2,3-diol With hydrogen bromide Reflux; 2: hydroquinone
参考文献
Mikhalitsyna, Elena A.; Tyurin, Vladimir S.; Nefedov, Sergey E.; Syrbu, Sergey A.; Semeikin, Aleksandr S.; Koifman, Oskar I.; Beletskaya, Irina P.
European Journal of Inorganic Chemistry, 2012 , # 36 p. 5979 - 5990
1: With sodium hydroxide; sodium hydrogensulfite in water T=50 - 65°C; 4 h; 2: With phosphoric acid in water T=45°C; pH=11; 3: With sulfuric acid in water T=55°C; pH=6.5 - 7.5; Product distribution / selectivity;
1: With sodium hydroxide in water T=50 - 65°C; 4 h; 2: With phosphoric acid in water T=45°C; pH=11; 3: With sulfuric acid in water T=55°C; pH=6.5 - 7.5; Product distribution / selectivity;
