1: 5 percent / Et3N; pyridine / 120 h / 20 °C 2: Na; MeOH / 100.8 h / 20 °C View Scheme
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Amberlyst 15 in tetrahydrofuran; hexane T=65 - 75°C;
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phosphoric acid in Petroleum ether T=30 - 35°C; 6 h;
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cyclic polyphosphate ester in chloroform 7 h; Ambient temperature;
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