in diethyl ether under Ar, stirring for 20 h at room temp.; filtration of ppt., washing with Et2O, drying in vac.; elem. anal.;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 566, p. 121 - 130
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反应条件
water in water Kinetics; in aq. acidic soln., 25°C, effect of nucleophilic reagents (SCN(1-), Cl(1-), CH3CO2(1-), pyridine, hydroxylamine or thiourea); spectrophotometry;