in neat (no solvent)
byproducts: methanol; org. compd. addn. gradually to Sn-compd. in evac. ampoule at room temp., after bulk methanol liberation reaction mixt. heating slowly to 125°C, then allowing to cool in air; recryst. (toluene/heptane); elem. anal.;
参考文献
Shcherbakov, V. I.; Stolyarova, N. E.; Trukhina, T. V.; Razuvaev, G. A.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1841 - 1843
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 2062 - 2064
Arndt, Matthias; Salih, Kifah S. M.; Fromm, Andreas; Goossen, Lukas J.; Menges, Fabian; Niedner-Schatteburg, Gereon
Journal of the American Chemical Society, 2011 , vol. 133, # 19 p. 7428 - 7449
Arndt, Matthias; Salih, Kifah S. M.; Fromm, Andreas; Goossen, Lukas J.; Menges, Fabian; Niedner-Schatteburg, Gereon
Journal of the American Chemical Society, 2011 , vol. 133, # 19 p. 7428 - 7449