1: C11H13PolS2 With n-butyllithium in tetrahydrofuran T=-35°C; 2 h; solid phase reaction; 2: butyraldehyde in tetrahydrofuran; Petroleum ether T=-35°C; solid phase reaction; 3: With N-bromosuccinmide in tetrahydrofuran; water
参考文献
Bertini, Vincenzo; Lucchesini, Francesco; Pocci, Marco; Alfei, Silvana; Idini, Barbara
Synlett, 2008 , # 8 p. 1141 - 1144
triethylamine; sodium bromide in N,N-dimethyl-formamide 6 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
