4-硝基苯基-β-D-硫代半乳糖苷合成路线 （共 6 条）
反应条件
sodium methylate in methanol 30 h; Ambient temperature;
参考文献
Cao; Meunier; Andersson; Letellier; Roy
Tetrahedron Asymmetry, 1994 , vol. 5, # 11 p. 2303 - 2312
反应条件
1: TBAHS; aq. Na2CO3 / CH2Cl2 / 3 h / 20 °C 2: NaOMe; MeOH View Scheme
参考文献
Cao; Meunier; Andersson; Letellier; Roy
Tetrahedron Asymmetry, 1994 , vol. 5, # 11 p. 2303 - 2312
反应条件
1: TBAHS; aq. Na2CO3 / CH2Cl2 / 3 h / 20 °C 2: NaOMe; MeOH View Scheme
参考文献
Giguere, Denis; Sato, Sachiko; St-Pierre, Christian; Sirois, Suzanne; Roy, Rene
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 6 p. 1668 - 1672
反应条件
1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 20 °C 2: sodium methylate / methanol / 20 °C View Scheme
参考文献
Ramos-Soriano, Javier; Niss, Ulf; Angulo, Jesus; Angulo, Manuel; Moreno-Vargas, Antonio J.; Carmona, Ana T.; Ohlson, Sten; Robina, Inmaculada
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17989 - 18003
反应条件
1: hydrogen bromide; acetic acid / dichloromethane / 2.5 h / 0 - 20 °C 2: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 20 °C 3: sodium methylate / methanol / 20 °C View Scheme
参考文献
Ramos-Soriano, Javier; Niss, Ulf; Angulo, Jesus; Angulo, Manuel; Moreno-Vargas, Antonio J.; Carmona, Ana T.; Ohlson, Sten; Robina, Inmaculada
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17989 - 18003
反应条件
Aspergillus oryzae β-thiogalactosidase T=40°C; Hydrolysis; pH=4.5; 0.166667 h; Product distribution; Further Variations:Reagents;
参考文献
Bioscience, biotechnology, and biochemistry, , vol. 64, # 4 p. 735 - 740
