N-(2-溴-5-甲氧基苯基)乙胺合成路线 （共 5 条）
反应条件
triethylamine in dichloromethane T=20°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 43, # 10 p. 1893 - 1895
反应条件
1: iron, acetic acid / ethanol / 2 h / 100 °C 2: pyridine / CH2Cl2 / 15 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 25 p. 5856 - 5866
反应条件
pyridine in dichloromethane 15 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 25 p. 5856 - 5866
反应条件
1: 91.7 percent / 48percent HBr, aq. sodium nitrite / H2O; dioxane / 36 h / 23 °C 2: iron, acetic acid / ethanol / 2 h / 100 °C 3: pyridine / CH2Cl2 / 15 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 25 p. 5856 - 5866
反应条件
1: With copper(l) iodide; K2S in N,N-dimethyl-formamide T=140°C; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C;
参考文献
Ma, Dawei; Xue, Peng; Jiang, Yongwen; Xie, Siwei; Zhang, Xiaojing; Dong, Jinhua
Angewandte Chemie, International Edition, 2009 , vol. 48, # 23 p. 4222 - 4225
