5-(2-乙基己基)-4H-噻吩并[3,4-c]吡咯-4,6(5h)-二酮合成路线 (共 3 条)
反应条件
1: thiophene-3,4-dicarboxylic acid With acetic anhydride T=140°C; 2: mono-2-ethylhexylamine in toluene 24 h; Reflux; 3: With thionyl chloride in toluene Reflux;
参考文献
Najari, Ahmed; Beaupre, Serge; Berrouard, Philippe; Zou, Yingping; Pouliot, Jean-Remi; Lepage-Perusse, Charlotte; Leclerc, Mario
Advanced Functional Materials, 2011 , vol. 21, # 4 p. 718 - 728
反应条件
thionyl chloride T=72°C; 3 h; Inert atmosphere;
参考文献
Piliego, Claudia; Holcombe, Thomas W.; Douglas, Jessica D.; Woo, Claire H.; Beaujuge, Pierre M.; Frechet, Jean M. J.
Journal of the American Chemical Society, 2010 , vol. 132, # 22 p. 7595 - 7597
反应条件
in acetic acid Inert atmosphereRefluxSchlenk technique;
参考文献
Feng, Quanyou; Zhang, Weiyi; Zhou, Gang; Wang, Zhong-Sheng
Chemistry - An Asian Journal, 2013 , vol. 8, # 1 p. 168 - 177