2,2,4-三甲基-7-[(E)-3-苯基丙-2-烯酰基]-1,4-苯并恶嗪-3-酮合成路线 (共 4 条)
反应条件
hydrogenchloride in ethanol 2 h; Ambient temperature;
参考文献
Moussavi, Ziaeddine; Lesieur, Daniel; Lespagnol, Charles; Sauzieres, Jacques; Olivier, Philippe
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 55 - 60
反应条件
1: 60 percent / NaOH 2: 75 percent / C2H5ONa / dimethylsulfoxide / 3 h / Ambient temperature 3: 65 percent / HCl gas / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Moussavi, Ziaeddine; Lesieur, Daniel; Lespagnol, Charles; Sauzieres, Jacques; Olivier, Philippe
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 55 - 60
反应条件
1: 70 percent / polyphosphoric acid 2: 60 percent / NaOH 3: 75 percent / C2H5ONa / dimethylsulfoxide / 3 h / Ambient temperature 4: 65 percent / HCl gas / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Moussavi, Ziaeddine; Lesieur, Daniel; Lespagnol, Charles; Sauzieres, Jacques; Olivier, Philippe
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 55 - 60
反应条件
1: 75 percent / C2H5ONa / dimethylsulfoxide / 3 h / Ambient temperature 2: 65 percent / HCl gas / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Moussavi, Ziaeddine; Lesieur, Daniel; Lespagnol, Charles; Sauzieres, Jacques; Olivier, Philippe
European Journal of Medicinal Chemistry, 1989 , vol. 24, p. 55 - 60