1: in tetrahydrofuran; diethyl ether T=-78°C; 3 h; 2: With lithium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=0°C; 7 h; Title compound not separated from byproducts;
参考文献
Reid, Gary P.; Brear, Kieron W.; Robins, David J.
Tetrahedron Asymmetry, 2004 , vol. 15, # 5 p. 793 - 801
1: in tetrahydrofuran; diethyl ether T=-78°C; 3 h; 2: With lithium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=0°C; 7 h; Title compound not separated from byproducts;
