(E)-3-对甲苯丙烯酸丁酯合成路线 （共 28 条）
反应条件
2,9-dimethyl-1,10-phenanthroline; p-benozquinone; palladium diacetate in acetonitrile
T=20°C; Heck reaction; 24 h;
参考文献
Lindh, Jonas; Enquist, Per-Anders; Pilotti, Ake; Nilsson, Peter; Larhed, Mats
Journal of Organic Chemistry, 2007 , vol. 72, # 21 p. 7957 - 7962
反应条件
sodium carbonate; PdCl2*di-(1-adamantyl)phosphine in N,N-dimethyl acetamide
T=140°C; Heck reaction; 20 h;
参考文献
Schnyder, Anita; Aemmer, Thomas; Indolese, Adriano F.; Pittelkow, Ulrich; Studer, Martin
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 5 p. 495 - 498
反应条件
Aliquatreg; 336; potassium carbonate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in xylene
T=140°C; Mizoroki-Heck reaction;
参考文献
Dubbaka, Srinivas Reddy; Vogel, Pierre
Chemistry - A European Journal, 2005 , vol. 11, # 9 p. 2633 - 2641
反应条件
1-tert-butyl-3-(2-(diphenylarsinyl)benzyl)-1H-imidazol-3-ium chloride; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in isobutyramide
T=60°C; Heck reaction; 20 h; Inert atmosphere;
参考文献
Stiemke, Frank; Gjikaj, Mimoza; Kaufmann, Dieter E.
Journal of Organometallic Chemistry, 2009 , vol. 694, # 1 p. 5 - 13
反应条件
copper diacetate; palladium diacetate in tetrahydrofuran; dimethyl sulfoxide
T=70°C; Heck Reaction; 6 h; stereoselective reaction;
参考文献
Hu, Sai; Xia, Ping; Cheng, Kai; Qi, Chenze
Applied Organometallic Chemistry, 2013 , vol. 27, # 3 p. 188 - 190
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2 in tetrahydrofuran
T=70°C; Mizoroki-Heck-type reaction; 24 h;
参考文献
Mori; Danda; Fujii; Hirabayashi; Osakada
Journal of the American Chemical Society, 2001 , vol. 123, # 43 p. 10774 - 10775
反应条件
C14H16N6; palladium diacetate; silver fluoride in N,N-dimethyl acetamide
T=60°C; Mizoroki-Heck type reaction; 24 h;
参考文献
Mino, Takashi; Shibuya, Masanori; Suzuki, Saori; Hirai, Kiminori; Sakamoto, Masami; Fujita, Tsutomu
Tetrahedron, 2012 , vol. 68, # 2 p. 429 - 432
反应条件
C14H16N6; palladium diacetate; silver fluoride in 1-methyl-pyrrolidin-2-one
T=60°C; Mizoroki-Heck type reaction; 24 h;
参考文献
Mino, Takashi; Shibuya, Masanori; Suzuki, Saori; Hirai, Kiminori; Sakamoto, Masami; Fujita, Tsutomu
Tetrahedron, 2012 , vol. 68, # 2 p. 429 - 432
反应条件
palladium diacetate; oxygen; sodium acetate in N,N-dimethyl-formamide
T=130°C; Heck olefination; 12 h;
参考文献
Hwang, Lee Kyoung; Na, Youngim; Lee, Junseong; Do, Youngkyu; Chang, Sukbok
Angewandte Chemie - International Edition, 2005 , vol. 44, # 38 p. 6166 - 6169
反应条件
potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride in N,N-dimethyl acetamide
T=140°C; Heck reaction; 11 h;
参考文献
Wang, Ai-E; Xie, Jian-Hua; Wang, Li-Xin; Zhou, Qi-Lin
Tetrahedron, 2005 , vol. 61, # 1 p. 259 - 266
