反应条件
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere
2: 4-(N,N-dimethlyamino)pyridine; triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 1 h / 0 - 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
INSTITUT CATALA D'INVESTIGACIO QUIMICA (ICIQ); ECHAVARREN PABLOS, Antonio Maria; MOLAWI, Kian; DELPONT, Nicolas, Pierre, Robert
Patent: WO2011/120886 A1, 2011 ;
