反应条件
1.1: POCl3 / 1,2-dichloro-ethane / 0 - 5 °C
1.2: 1,2-dichloro-ethane / Heating
1.3: NaOAc*3H2O / 1,2-dichloro-ethane; H2O / Heating
2.1: 39.5 g / aq. NaOH / 3 h / Heating
View Scheme
参考文献
Miller, Raya; Olsson, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1981 , vol. 35, # 4 p. 303 - 304