1-环戊基-1H-吡唑-4-硼酸频那醇酯合成路线 (共 2 条)
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in dimethyl sulfoxide T=100°C; 12 h; Inert atmosphereSealed tube;
参考文献
ORION CORPORATION; LINNANEN, Tero; WOHLFAHRT, Gerd; NANDURI, Srinivas; UJJINAMATADA, Ravi; RAJAGOPALAN, Srinivasan; MUKHERJEE, Subhendu
Patent: WO2013/53983 A1, 2013 ;
Location in patent: Page/Page column 48 ;
反应条件
caesium carbonate in acetonitrile T=90°C; 2 h;
参考文献
GLAXO GROUP LIMITED; Atkinson, Francis Louis; Atkinson, Stephen John; Barker, Michael David; Douault, Clement; Garton, Neil Stuart; Liddle, John; Patel, Vipulkumar Kantibhai; Preston, Alexander G.; Shipley, Tracy Jane; Wilson, David Matthew; Watson, Robert J.
Patent: US2014/5188 A1, 2014 ;
Location in patent: Paragraph 0571; 0572; 0573 ;