1: 434 mg / DIBAL / tetrahydrofuran / 0.5 h / -78 °C
2: ethanol / 2 h / Heating
3: KOH / ethanol; H2O / 10 h / Heating
4: camphor-10-sulfonic acid / 12 h / Ambient temperature
View Scheme
参考文献
Toyota, Masahiro; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 5 p. 547 - 552
1: ethanol / 2 h / Heating
2: KOH / ethanol; H2O / 10 h / Heating
3: camphor-10-sulfonic acid / 12 h / Ambient temperature
View Scheme
参考文献
Toyota, Masahiro; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 5 p. 547 - 552