N-叔丁氧羰基-L-谷氨酸 5-芴甲基酯合成路线 (共 5 条)
反应条件
sodium carbonate in tetrahydrofuran; water 1) 0 deg C, 15 min (pH 9.5) 2) 25 deg C, 2 h;
参考文献
Albericio, F.; Nicolas, E.; Rizo, J.; Ruiz-Gayo, M.; Pedroso, E.; Giralt, E.
Synthesis, 1990 , # 2 p. 119 - 122
反应条件
1: L-glutamic acid δ-fluorenylmethyl ester hydrochloride With sodium carbonate 2: di-tert-butyl dicarbonate
参考文献
Crich, David; Sana, Kasinath
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7383 - 7388
反应条件
in 1,4-dioxane; water
参考文献
Belshaw; Adamson; Lajoie
Synthetic Communications, 1992 , vol. 22, # 7 p. 1001 - 1005
反应条件
1: 65 percent / sodium sulfate, tetrafluoroboric acid diethyletherate / tetrahydrofuran / 14 h / Ambient temperature 2: 89 percent / H2O; dioxane View Scheme
参考文献
Synthetic Communications, , vol. 22, # 7 p. 1001 - 1005
反应条件
1: 65 percent / sodium sulfate, tetrafluoroboric acid diethyletherate / tetrahydrofuran / 14 h / Ambient temperature 2: 89 percent / H2O; dioxane View Scheme
参考文献
Synthetic Communications, , vol. 22, # 7 p. 1001 - 1005