1-(5-溴-4-氯-2-噻吩基)乙酮合成路线 （共 4 条）
反应条件
aluminium trichloride; bromine in chloroform 2 h; Heating;
参考文献
Stanetty, Peter; Puschautz, Erhard; Friedbacher, Gernot
Monatshefte fuer Chemie, 1989 , vol. 120, p. 53 - 63
反应条件
1: 96 percent / 1.16M Cl2, AlCl3 / CHCl3; CCl4 / 1.5 h / 30 °C 2: 81 percent / Zn / H2O; acetic acid / 2.5 h / Heating 3: 95 percent / Br2, AlCl3 / CHCl3 / 2 h / Heating View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 120, p. 53 - 63
反应条件
1: 81 percent / Zn / H2O; acetic acid / 2.5 h / Heating 2: 95 percent / Br2, AlCl3 / CHCl3 / 2 h / Heating View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 120, p. 53 - 63
反应条件
sodium hydroxide; water; bromine T=0°C; 12 h;
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2007/76423 A2, 2007 ;
Location in patent: Page/Page column 142 ;
WO 2007/076423 A2
