2-(4-(二氟甲基)苯基)-4,4,5,5-四甲基-1,3,2-二噁硼烷合成路线 (共 2 条)
反应条件
potassium acetate; palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] in 1,4-dioxane T=100°C; 18 h;
参考文献
Pfizer Inc.
Patent: US2012/214791 A1, 2012 ;
Location in patent: Page/Page column 27 ;
US 20120214791 A1
反应条件
1: diethylamino-sulfur trifluoride / dichloromethane / 19 h / 20 °C / Reflux 2: potassium acetate / palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] / 1,4-dioxane / 18 h / 100 °C View Scheme
参考文献
Pfizer Inc.
Patent: US2012/214791 A1, 2012 ;
US 20120214791 A1