4-羟基苯基4-(十二基氧基)苯甲酸盐合成路线 （共 13 条）
反应条件
palladium 10 on activated carbon; hydrogen in tetrahydrofuran
T=20°C;
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
反应条件
triethylamine; palladium monocarbide in tetrahydrofuran
参考文献
Mitsubishi Rayon Co., Ltd.
Patent: US4925591 A1, 1990 ;
反应条件
1: thionyl chloride / 3 h / Heating
2: CH2Cl2; pyridine
View Scheme
参考文献
Vajda, Aniko; Kaspar, Miroslav; Hamplova, Vera; Pakhomov, Ser-Gei A.; Vanek, Premysl; Bubnov, Alexei; Fodor-Csorba, Katalin; Eber, Nandor
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 365, p. 569 - 580
反应条件
1: pyridine
2: H2 / Pd/C / acetic acid
View Scheme
参考文献
Tinh, Nguyen Huu; Salleneuve, C.; Babeau, A.; Galvan, J. M.; Destrade, C.
Molecular Crystals and Liquid Crystals (1969-1991), 1987 , vol. 151, p. 147 - 154
反应条件
1: dicyclohexylcarbodiimide, N,N-dimethylaminopyridine / CH2Cl2 / 24 h / Ambient temperature
2: H2, Et3N / 10percent Pd/C / tetrahydrofuran / Ambient temperature
View Scheme
参考文献
Rowe, Kathryn E.; Bruce, Duncan W.
Journal of Materials Chemistry, 1998 , vol. 8, # 2 p. 331 - 341
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 90 °C
2: potassium hydroxide / ethanol; water / 2 h / |Reflux
3: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
4: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
5: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
参考文献
Achten, Remko; Marcelis, Antonius T.M.; Koudijs, Arie; Sudhoelter, Ernst J.R.
Molecular Crystals and Liquid Crystals, 2004 , vol. 411, p. 177/[1219]-184/[1226]
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 90 °C
2: potassium hydroxide / ethanol; water / 2 h / |Reflux
3: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
4: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
5: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
反应条件
1: potassium hydroxide / ethanol; water / 2 h / |Reflux
2: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
3: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
4: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
反应条件
1: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
2: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
