4-羟基苯基4-(十二基氧基)苯甲酸盐合成路线 （共 13 条）
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 90 °C
2: potassium hydroxide / ethanol; water / 2 h / |Reflux
3: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
4: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
5: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
反应条件
1: potassium hydroxide / ethanol; water / 2 h / |Reflux
2: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
3: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
4: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
反应条件
1: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / |Reflux
2: triethylamine / butanone / 4.5 h / 0 °C / |Cooling with ice
3: palladium 10 on activated carbon; hydrogen / tetrahydrofuran / 20 °C
View Scheme
参考文献
Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy
Molecular Crystals and Liquid Crystals, 2013 , vol. 582, # 1 p. 1 - 14
