2,5-双(辛氧基)对苯二甲醛合成路线 （共 4 条）
反应条件
1: 2,5-diiodo-1,4-bis(n-octyloxy)benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78°C; 2 h;
参考文献
Liao, Jian; Wang, Qing
Macromolecules, 2004 , vol. 37, # 18 p. 7061 - 7063
反应条件
n-butyllithium in diethyl ether; n-heptane T=10 - 15°C; Bouveault formylation; 1.5 h;
参考文献
Egbe, Daniel Ayuk Mbi; Cornelia, Bader; Nowotny, Juergen; Guenther, Wolfgang; Klemm, Elisabeth
Macromolecules, 2003 , vol. 36, # 15 p. 5459 - 5469
反应条件
n-butyllithium in diethyl ether T=0 - 20°C; 12 h;
参考文献
Kim, Ji-Hoon; Mi, Dongbo; Kang, In-Nam; Shin, Won Suk; Yoon, Sung Cheol; Moon, Sang-Jin; Lee, Changjin; Lee, Jin-Kyun; Hwang, Do-Hoon
Journal of Nanoscience and Nanotechnology, 2011 , vol. 11, # 7 p. 5876 - 5882
反应条件
1.1: sodium acetate; bromine / acetic acid / 20 °C 2.1: n-butyllithium / tetrahydrofuran / 3 h / -78 °C 2.2: 3 h / -78 - 20 °C View Scheme
参考文献
Gatri, Rafik; Ouerfelli, Ines; Efrit, Mohamed Lofti; Serein-Spirau, Francoise; Lere-Porte, Jean-Pierre; Valvin, Pierre; Roisnel, Thierry; Bivaud, Sebastien; Akdas-Kilig, Huriye; Fillaut, Jean-Luc
Organometallics, 2014 , vol. 33, # 3 p. 665 - 676
