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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
123533-11-9
合成路线
（共 11 条）
123533-10-8
→
反应条件
123533-11-9
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C;
参考文献
Faraj; Maillard; Lemaitre; Letellier; Frappier; Florent; Grierson; Monneret; Zerial
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 2 p. 141 - 148
628-36-4
二甲酰肼
+
52450-18-7
3’-氨基-2’,3’-双脱氧胸苷
→
反应条件
123533-11-9
反应条件
pyridine Heatingovernight;
参考文献
Wigerinck, Piet; Aerschot, Arthur Van; Janssen, Gerard; Claes, Paul; Balzarini, Jan; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 2 p. 868 - 873
123556-91-2
→
反应条件
123533-11-9
反应条件
1: 85 percent / i-Pr2NEt / dimethylformamide / 0.5 h / 0 °C 2: 90 percent / Bu4NF / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 27, # 2 p. 141 - 148
123533-06-2
→
反应条件
123533-11-9
反应条件
1: 85 percent / SnCl2 / methanol / 1 h / Ambient temperature 2: 85 percent / i-Pr2NEt / dimethylformamide / 0.5 h / 0 °C 3: 90 percent / Bu4NF / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Maillard, Michel; Faraj, Abdesslem; Frappier, Francois; Florent, Jean-Claude; Grierson, David S.; Monneret, Claude
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1955 - 1958
124355-26-6
→
反应条件
123533-11-9
反应条件
1: dimethylformamide / 72 h / 100 °C 2: AcOH / methanol / 1 h / 100 °C View Scheme
参考文献
Wigerinck, Piet; Aerschot, Arthur Van; Janssen, Gerard; Claes, Paul; Balzarini, Jan; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 2 p. 868 - 873
124355-25-5
→
反应条件
123533-11-9
反应条件
1: methanol 2: dimethylformamide / 72 h / 100 °C 3: AcOH / methanol / 1 h / 100 °C View Scheme
参考文献
Wigerinck, Piet; Aerschot, Arthur Van; Janssen, Gerard; Claes, Paul; Balzarini, Jan; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 2 p. 868 - 873
52450-18-7
3’-氨基-2’,3’-双脱氧胸苷
+
2258-42-6
甲乙酐
→
反应条件
123533-11-9
反应条件
in pyridine 72 h; Ambient temperature;
参考文献
Motawia; Pedersen
Archiv der Pharmazie, 1990 , vol. 323, # 12 p. 971 - 975
123533-05-1
→
反应条件
123533-11-9
反应条件
1: 85 percent / NaN3 / dimethylformamide / 120 °C 2: 85 percent / SnCl2 / methanol 3: 90 percent / ethyldiisopropylamine / dimethylformamide / 0 deg C to 20 deg C 4: 90 percent / Bu4NF / tetrahydrofuran / 20 °C View Scheme
参考文献
Maillard, Michel; Faraj, Abdesslem; Frappier, Francois; Florent, Jean-Claude; Grierson, David S.; Monneret, Claude
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1955 - 1958
123533-02-8
→
反应条件
123533-11-9
反应条件
1: 95 percent / pyridine / 0 °C 2: 98 percent / DBU / 2 h / Heating 3: 85 percent / NaN3 / dimethylformamide / 120 °C 4: 85 percent / SnCl2 / methanol 5: 90 percent / ethyldiisopropylamine / dimethylformamide / 0 deg C to 20 deg C 6: 90 percent / Bu4NF / tetrahydrofuran / 20 °C View Scheme
参考文献
Maillard, Michel; Faraj, Abdesslem; Frappier, Francois; Florent, Jean-Claude; Grierson, David S.; Monneret, Claude
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1955 - 1958
123533-04-0
→
反应条件
123533-11-9
反应条件
1: 98 percent / DBU / 2 h / Heating 2: 85 percent / NaN3 / dimethylformamide / 120 °C 3: 85 percent / SnCl2 / methanol 4: 90 percent / ethyldiisopropylamine / dimethylformamide / 0 deg C to 20 deg C 5: 90 percent / Bu4NF / tetrahydrofuran / 20 °C View Scheme
参考文献
Maillard, Michel; Faraj, Abdesslem; Frappier, Francois; Florent, Jean-Claude; Grierson, David S.; Monneret, Claude
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1955 - 1958
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