孕甾-5-烯-3,20-二酮合成路线 （共 13 条）
反应条件
sulfuric acid; dihydrogen peroxide; sodium tungstate in water; acetonitrile T=80°C; 5 h;
参考文献
Bhati, Nishi; Sarma, Kuladip; Goswami, Amrit
Synthetic Communications, 2008 , vol. 38, # 9 p. 1416 - 1424
反应条件
lt;MoO(O2)2C5H4N(O)COOgt;Bu4N in 1,2-dichloro-ethane T=50°C; 10 h;
参考文献
Bortolini, O.; Campestrini, S.; Furia, F. Di; Modena, G.; Valle, G.
Journal of Organic Chemistry, 1987 , vol. 52, # 24 p. 5467 - 5469
反应条件
potassium hydroxide; sodium hydrogencarbonate; acetic acid in ethylene glycol dimethyl ether 15 h; Ambient temperature;
参考文献
D'Incan, E.; Viout, P.
Tetrahedron, 1984 , vol. 40, # 18 p. 3421 - 3424
反应条件
jones reagent in diethyl ether 0.25 h; Heating;
参考文献
Solaja, Bogdan A.; Mili, Dragana R.; Do, Ljiljana I.
Steroids, 1994 , vol. 59, # 5 p. 330 - 334
反应条件
tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide in dichloromethane; acetonitrile 8 h;
参考文献
Acosta, C. Kirk; Rao, Pemmaraju N.; Kim, Hyun K.
Steroids, 1993 , vol. 58, # 5 p. 205 - 208
反应条件
hydrogenchloride; sodium hydroxide; oxygen; tin(ll) chloride; lithium diisopropyl amide Yield given. Multistep reaction;
参考文献
Freerksen, Robert W.; Selikson, Sandra J.; Wroble, Randall R.; Kyler, S. Keith; Watt, David S.
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4087 - 4096
反应条件
chromic acid in acetone T=0°C; 0.0666667 h; Title compound not separated from byproducts;
参考文献
Herl, Vanessa; Frankenstein, Joerdis; Meitinger, Nadine; Mueller-Uri, Frieder; Kreis, Wolfgang
Planta Medica, 2007 , vol. 73, # 7 p. 704 - 710
反应条件
(i) aq. AcOH, (ii) aq. NaOH; Multistep reaction;
参考文献
Bucourt,R.; Dube,J.
Bulletin de la Societe Chimique de France, 1974 , p. 479 - 483
参考文献
Westphal; Schmidt-Thome
Chemische Berichte, 1936 , vol. 69, p. 889,892
参考文献
Westphal; Schmidt-Thome
Chemische Berichte, 1936 , vol. 69, p. 889,892
