6-(溴甲基)-2-氯喹啉合成路线 (共 2 条)
反应条件
trichlorophosphate in trichlorophosphate T=60°C; 17 h;
参考文献
US2004/102450 A1, ;
Page/Page column 70 ;
反应条件
1: With 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in ethanol; water
1 h; Heating / reflux;
2: With hydrogenchloride; water in ethanol
T=20°C; 0.583333 h; Heating / reflux;
参考文献
GENELABS TECHNOLOGIES, INC.
Patent: WO2008/8912 A1, 2008 ;
Location in patent: Page/Page column 87; 99-100 ;