2-溴-6-(1H-吡唑-1-基)吡啶合成路线 (共 3 条)
反应条件
potassium tert-butylate in 1,4-dioxane 48 h; Reflux;
参考文献
Huang, Kuo-Wei; Chen, Tao; He, Lipeng; Gong, Dirong; Jia, Weiguo; Yao, Liangfeng
Patent: US2012/323007 A1, 2012 ;
Location in patent: Page/Page column 13 ;
反应条件
potassium tert-butylate in 1,4-dioxane T=100°C; 48 h; Schlenk techniqueInert atmosphere;
参考文献
Heider, Silvio; Petzold, Holm; Chastanet, Guillaume; Schlamp, Stephan; Rueffer, Tobias; Weber, Birgit; Letard, Jean-Francois
Dalton Transactions, 2013 , vol. 42, # 24 p. 8575 - 8584
反应条件
in diethylene glycol dimethyl ether T=60°C; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 17 p. 4992 - 4994