反应条件
1: 49 percent / NH4Cl, NH4OH / propan-2-ol / 15 h / 25 °C
2: 64 percent / PCC / CH2Cl2 / 11 h / Heating
3: 88 percent / dimethylformamide / 15 h / 25 °C
4: 99 percent / diethyl ether; ethyl acetate / 15 h / 0 °C
5: 62 percent / (i-Bu)2AlH / CH2Cl2 / 3 h / 0 °C
6: PCC, NaOAc / CH2Cl2 / 13 h / 25 °C
7: NaN3 / LiCl / dimethylformamide / 15 h / 25 °C
8: 94 percent / diethyl ether / 3 h / 25 °C
9: 2.) NaBH3CN / 1.) Et2O, reflux, 2 h, 2.) MeOH, 25 deg C, 1 h
10: NaBH4 / methanol; H2O / 3 h / 0 °C
11: 50percent aq. TFA / 0.33 h / 0 °C
View Scheme
参考文献
White; Cammack; Sakuma
Journal of the American Chemical Society, 1989 , vol. 111, # 24 p. 8970 - 8972
