您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
123662-55-5
合成路线
（共 8 条）
123662-55-5
→
反应条件
123663-49-0
艾拉莫德
反应条件
1: H2 / 5 percent Pd/C / acetic acid / 1 h / 40 - 45 °C / 760 Torr 2: 97 percent / Br2 / CHCl3 / 0.5 h / 25 - 30 °C 3: 80 percent / NaN3; DMF / 1 h / 70 - 75 °C 4: 73 percent / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Inaba, Takihiro; Tanaka, Keiichi; Takeno, Ryuko; Nagaki, Hideyoshi; Yoshida, Chosaku; Takano, Shuntaro
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 1 p. 131 - 139
123664-52-8
+
109-94-4
甲酸乙酯
→
反应条件
123662-55-5
反应条件
hydrogenchloride in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water; acetic acid; toluene
参考文献
Toyama Chemical Company, Ltd.
Patent: US4954518 A1, 1990 ;
84594-95-6
→
反应条件
123662-55-5
反应条件
1: 72 percent / 4N aq. HCl; Fe / ethanol / 0.33 h / 65 - 70 °C 2: 82 percent / pyridine / 1 h / 20 °C 3: 84 percent / aluminum chloride / CH2Cl2 / 1 h / 15 - 20 °C 4: 70 percent aq. HClO4 / 1 h / 20 °C 5: H2O / 0.08 h / Heating View Scheme
参考文献
Inaba, Takihiro; Tanaka, Keiichi; Takeno, Ryuko; Nagaki, Hideyoshi; Yoshida, Chosaku; Takano, Shuntaro
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 1 p. 131 - 139
76838-72-7
3-氨基-4-苯氧基苯甲醚
→
反应条件
123662-55-5
反应条件
1: 82 percent / pyridine / 1 h / 20 °C 2: 84 percent / aluminum chloride / CH2Cl2 / 1 h / 15 - 20 °C 3: 70 percent aq. HClO4 / 1 h / 20 °C 4: H2O / 0.08 h / Heating View Scheme
参考文献
Inaba, Takihiro; Tanaka, Keiichi; Takeno, Ryuko; Nagaki, Hideyoshi; Yoshida, Chosaku; Takano, Shuntaro
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 1 p. 131 - 139
10298-80-3
4-氯-3-硝基苯甲醚
→
反应条件
123662-55-5
反应条件
1: 84 percent / potassium tert-butoxide / dimethylformamide / 4 h / 110 °C 2: 72 percent / 4N aq. HCl; Fe / ethanol / 0.33 h / 65 - 70 °C 3: 82 percent / pyridine / 1 h / 20 °C 4: 84 percent / aluminum chloride / CH2Cl2 / 1 h / 15 - 20 °C 5: 70 percent aq. HClO4 / 1 h / 20 °C 6: H2O / 0.08 h / Heating View Scheme
参考文献
Inaba, Takihiro; Tanaka, Keiichi; Takeno, Ryuko; Nagaki, Hideyoshi; Yoshida, Chosaku; Takano, Shuntaro
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 1 p. 131 - 139
123664-84-6
→
反应条件
123662-55-5
反应条件
1: 84 percent / aluminum chloride / CH2Cl2 / 1 h / 15 - 20 °C 2: 70 percent aq. HClO4 / 1 h / 20 °C 3: H2O / 0.08 h / Heating View Scheme
参考文献
Inaba, Takihiro; Tanaka, Keiichi; Takeno, Ryuko; Nagaki, Hideyoshi; Yoshida, Chosaku; Takano, Shuntaro
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 1 p. 131 - 139
108-95-2
苯酚
→
反应条件
123662-55-5
反应条件
1: 84 percent / potassium tert-butoxide / dimethylformamide / 4 h / 110 °C 2: 72 percent / 4N aq. HCl; Fe / ethanol / 0.33 h / 65 - 70 °C 3: 82 percent / pyridine / 1 h / 20 °C 4: 84 percent / aluminum chloride / CH2Cl2 / 1 h / 15 - 20 °C 5: 70 percent aq. HClO4 / 1 h / 20 °C 6: H2O / 0.08 h / Heating View Scheme
参考文献
Inaba, Takihiro; Tanaka, Keiichi; Takeno, Ryuko; Nagaki, Hideyoshi; Yoshida, Chosaku; Takano, Shuntaro
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 1 p. 131 - 139
123664-52-8
→
反应条件
123662-55-5
反应条件
1: 70 percent aq. HClO4 / 1 h / 20 °C 2: H2O / 0.08 h / Heating View Scheme
参考文献
Inaba, Takihiro; Tanaka, Keiichi; Takeno, Ryuko; Nagaki, Hideyoshi; Yoshida, Chosaku; Takano, Shuntaro
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 1 p. 131 - 139
