4-甲基-苯乙酮(2,4-二硝基苯基)腙合成路线 （共 4 条）
反应条件
1: 4-methyl-styrene With dichloro bis(acetonitrile) palladium(II); water; p-benozquinone; tert-butyl alcohol T=85°C; Wacker oxidation; 1 h; 2: (2,4-dinitro-phenyl)-hydrazine in tert-butyl alcohol T=30°C; regioselective reaction;
参考文献
Teo, Peili; Wickens, Zachary K.; Dong, Guangbin; Grubbs, Robert H.
Organic Letters, 2012 , vol. 14, # 13 p. 3237 - 3239
参考文献
Roberts; Green
Journal of the American Chemical Society, 1946 , vol. 68, p. 214
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Tarbell; Fukushima
Journal of the American Chemical Society, 1946 , vol. 68, p. 1456,1458
Organic Syntheses, 1955 , vol. Coll. Vol. III, p. 809
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Naves
Helvetica Chimica Acta, 1948 , vol. 31, p. 44,47
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Ferrante; Bloom
American Journal of Pharmacy and the Sciences Supporting Public Health (1937-1978), 1933 , vol. 105, p. 381,384
反应条件
sulfuric acid; nitric acid Behandeln des Reaktionsprodukts mit <2,4-Dinitro-phenyl>-hydrazin-sulfat in Aethanol;
参考文献
Brady; Day
Journal of the Chemical Society, 1934 , p. 114,119
反应条件
aluminum oxide; potassium permanganate T=20°C; 1 h;
参考文献
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, , vol. 44, # 7 p. 1392 - 1394
