反应条件
1: 96 percent / acetonitrile / 48 h / Heating
2: 1) BuLi 2) HMPA / 1) THF, -78 deg C, 0.5 h, 2) THF, -78 deg C, 2 h
3: 100 percent / LiAlH4 / tetrahydrofuran / 0.17 h / 25 °C
4: 100 percent / 1percent aq. FeCl3 / benzene / 0.25 h
View Scheme
参考文献
Sargent, Melvyn V.; Wangchareontrakul, Sirichai
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 5 p. 1429 - 1434