(9CI)-甲氧基三甲基-脲合成路线 (共 7 条)
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=-20 - 20°C;
参考文献
Hlasta, Dennis J.; Court, John J.
Tetrahedron Letters, 1989 , vol. 30, # 14 p. 1773 - 1776
反应条件
in tetrahydrofuran; diethyl ether; cyclohexane 1) from -78 deg C to 0 deg C, 3 h; 2) from 0 deg C to room temperature, 1.5 h;
参考文献
Hlasta, Dennis J.; Court, John J.
Tetrahedron Letters, 1989 , vol. 30, # 14 p. 1773 - 1776
参考文献
Tetrahedron Letters, , vol. 30, # 14 p. 1773 - 1776
反应条件
in tetrahydrofuran; diethyl ether; cyclohexane T=-78°C; 1 h;
参考文献
Hlasta, Dennis J.; Court, John J.
Tetrahedron Letters, 1989 , vol. 30, # 14 p. 1773 - 1776
参考文献
Tetrahedron Letters, , vol. 30, # 14 p. 1773 - 1776
反应条件
in tetrahydrofuran; diethyl ether; cyclohexane 1) -78 deg C, 30 min; 2) from -78 deg C to room temperature, 5 h;
参考文献
Hlasta, Dennis J.; Court, John J.
Tetrahedron Letters, 1989 , vol. 30, # 14 p. 1773 - 1776
反应条件
in tetrahydrofuran 1) from -78 deg C to -20 deg C, 1 h; 2) from -78 deg C to room temperature, 1.5 h;
参考文献
Hlasta, Dennis J.; Court, John J.
Tetrahedron Letters, 1989 , vol. 30, # 14 p. 1773 - 1776