1-Boc-1,2,3,4-四氢喹啉-2-羧酸合成路线 (共 3 条)
反应条件
sodium hydroxide in tert-butyl alcohol 24 h; Ambient temperaturepH at 9.5;
参考文献
Journal of Organic Chemistry, , vol. 55, # 2 p. 738 - 741
反应条件
1: 81 percent / hydrogen / platinum oxide / acetic acid / 2 h / 60 °C / 3102.9 Torr 2: 2 N NaOH / 2-methyl-propan-2-ol / 24 h / Ambient temperature; pH at 9.5 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 2 p. 738 - 741
反应条件
1: platinum(IV) oxide; hydrogen / methanol / 2.5 h 2: triethylamine / dichloromethane / 20 °C View Scheme