反应条件
1: diisobutylaluminum hydride / CH2Cl2 / 3 h / 0 °C
2: 95 percent / pyridine / CH2Cl2 / 0.5 h / 0 °C
3: 30 percent / NaH, 18-crown-6 (3 equiv. each) / dimethylformamide / 18 h / 0 °C
4: 79 percent / trifluoroacetic acid / H2O / 3 h / 50 °C
View Scheme
参考文献
Wolfe, Michael S.; Anderson, Blake L.; Borcherding, David R.; Borchardt, Ronald T.
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4712 - 4717
