2-(3-硝基吡啶-2-基)乙腈合成路线 （共 5 条）
反应条件
1: 67 percent / NaOH / dimethylformamide / 1 h / 10 - 25 °C 2: 80 percent / hydrochloric acid / H2O / 1 h / Heating View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 71, # 7 p. 1076 - 1087
反应条件
1: 22 percent / HNO3; sulfuric acid / H2O / 20 - 80 °C 2: 62 percent / phosphorus pentachloride; phosphoryl chloride / 1 h / Heating 3: 67 percent / NaOH / dimethylformamide / 1 h / 10 - 25 °C 4: 80 percent / hydrochloric acid / H2O / 1 h / Heating View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 71, # 7 p. 1076 - 1087
反应条件
1: 62 percent / phosphorus pentachloride; phosphoryl chloride / 1 h / Heating 2: 67 percent / NaOH / dimethylformamide / 1 h / 10 - 25 °C 3: 80 percent / hydrochloric acid / H2O / 1 h / Heating View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 71, # 7 p. 1076 - 1087
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 24 h;
参考文献
Yamawaki, Kenji; Nomura, Takashi; Yasukata, Tatsuro; Uotani, Koichi; Miwa, Hideaki; Takeda, Kei; Nishitani, Yasuhiro
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 21 p. 6716 - 6732
反应条件
1: With palladium diacetate; dimethyl sulfoxide; trifluoroacetic acid T=90°C; 24 h; 2: With iron T=90°C; 2 h;
参考文献
Jadhav, Jagannath; Gaikwad, Vipul; Kurane, Rajanikant; Salunkhe, Rajashri; Rashinkar, Gajanan
Synlett, 2012 , vol. 23, # 17 p. 2511 - 2515,5
Title/Abstract Full Text Show Details
Jadhav, Jagannath; Gaikwad, Vipul; Kurane, Rajanikant; Salunkhe, Rajashri; Rashinkar, Gajanan
Synlett, 2012 , vol. 23, # 17 p. 2511 - 2515
