PPh3 in acetonitrile Electrolysis; Hg-cathode, Zn- or Cd-anode sepd. by sinter, 5.4 V;
参考文献
Cooksey, Brian G.; Gorham, John D.; Morris, John H.; Kane, Lorna
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 141 - 144
in dichloromethane 20°C, 72 h; filtered. evapd. to dryness;
参考文献
Greenwood, Norman N.; Kennedy, John D.; Reed, David
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , # 1 p. 196 - 200
in dichloromethane 23°C, 24 h; filtered, evapd. in vac., fractional crystn. from benzene/ether and dichloromethane/ether;
参考文献
Greenwood, Norman N.; Kennedy, John D.; Reed, David
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , # 1 p. 196 - 200