titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate in dichloromethane 4 Angstroem molecular sieves; 1.)-20 deg C, 0.5 h, 2.) -10 deg C, 29 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gao, Yun; Hanson, Robert M.; Klunder, Janice M.; Ko, Soo Y.; Masamune, Hiroko; Sharpless, K. Barry
Journal of the American Chemical Society, 1987 , vol. 109, # 19 p. 5765 - 5780
