(4-羟基甲基苄基)-氨基甲酸叔丁酯合成路线 (共 23 条)
反应条件
tetrachloromethane; triphenylphosphine in dichloromethane T=20°C; Substitution; 24 h;
参考文献
Yu, Chongxi; Taylor, John W.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 1 p. 161 - 175
反应条件
Dess-Martin periodane in dichloromethane T=-78 - 20°C; 3 h;
参考文献
LIGHTSHIP MEDICAL LIMITED; JAMES, Tony; BARWELL, Nicholas, Paul
Patent: WO2012/95628 A1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
T=0 - 20°C; 14 h;
参考文献
Solladie, Nathalie; Walther, Mathieu E.; Herschbach, Haiko; Leize, Emmanuelle; Dorsselaer, Alain Van; Duarte, Teresa M. Figueira; Nierengarten, Jean-Francois
Tetrahedron, 2006 , vol. 62, # 9 p. 1979 - 1987